cloud point extraction of pper

Cloud point extraction for the determination of copper ...

Feb 11, 2008  A cloud point extraction procedure was presented for the preconcentration of copper, nickel and cobalt ions in various samples. After complexation with methyl-2-pyridylketone oxime (MPKO) in basic medium, analyte ions are quantitatively extracted to the phase rich in Triton X-114 following centrifugation. 1.0 mol L −1 HNO 3 nitric acid in methanol was added to

The cloud point extraction of copper(II) with ...

Mar 10, 2003  The possibility to use monocarboxylic acids and their mixtures with amines for copper concentrating by the way of micellar extraction at cloud point t

Study on the Cloud Point Extraction of Copper(II) from an ...

Dec 01, 2009  Removal of Copper(II) from a Concentrated Sulphate Medium by Cloud Point Extraction Using an N,N′-Bis(salicylaldehyde)Ethylenediimine Di-Schiff Base Chelating Ligand. Journal of Surfactants and Detergents 2014 , 17 (1) , 27-35.

Cloud Point Extraction of Copper, Lead, Cadmium, and Iron ...

Nov 27, 2019  A cloud point extraction procedure was optimized for the separation and preconcentration of lead(II), cadmium(II), copper(II), and iron(III) ions in We use cookies to enhance your experience on our website.By continuing to use our website, you are agreeing to our use of cookies.

Cloud Point Extraction as a Procedure of Separation and ...

Cloud point extraction for the copper species was prepared at different buffered pH solutions. The separation of by copper ion cloud point extractioninvolves prior formation of a complex with sufficient hydrophobic and the Amoxicillin drug to be extracted into the small volume of the surfactant-rich phase. ...

Cloud point extraction and flame atomic absorption ...

Jun 15, 2009  Cloud point extraction was used with lipophilic Schiff base N,N′-bis(2-hydroxyacetophenone)-1,2-propanediimine (L) as a pre-concentration step prior to flame atomic absorption spectrometry determination of trace amounts of copper in water samples.The process is based upon the formation of Cu(II)/L complexes soluble in a micellar phase composed by

Cloud Point Extraction of Trace Amounts of Copper and Its ...

N. Baghban et al., Cloud Point Extraction of Trace Amounts of Copper 87 Croat. Chem. Acta 85 (2012) 85. Rice Flour Preparation One gram of rice flour was placed in a 100 mL beaker, 7 mL ...

Study on the Cloud Point Extraction of Copper(II) from an ...

In the present work, cloud point extraction process is used with bidentate Schiff base chelating ligand, Nsalicylideneaniline (SA or HL), to extract and separate copper (II)

Development of a cloud-point extraction method for copper ...

Development of a cloud-point extraction method for copper and nickel determination in food samples

Me-BTABr reagent in cloud point extraction for ...

The present paper describes a new cloud point extraction and preconcentration method for copper by the use of 2-[2´-(6-methyl-benzothiazolylazo)]-4-bromophenol (Me-BTABr) reagent as a complexing agent prior to flame atomic absorption spectrometric determination of this metal.

Study on the Cloud Point Extraction of Copper(II) from an ...

Dec 01, 2009  Removal of Copper(II) from a Concentrated Sulphate Medium by Cloud Point Extraction Using an N,N′-Bis(salicylaldehyde)Ethylenediimine Di-Schiff Base Chelating Ligand. Journal of Surfactants and Detergents 2014 , 17 (1) , 27-35.

Cloud Point Extraction of Copper, Lead, Cadmium, and Iron ...

A cloud point extraction procedure was optimized for the separation and preconcentration of lead(II), cadmium(II), copper(II), and iron(III) ions in We use cookies to enhance your experience on our website.By continuing to use our website, you are agreeing to our use of cookies.

Cloud point extraction for the determination of copper in ...

A simple cloud point extraction procedure is presented for the preconcentration of copper in various samples. After complexation by 4-hydroxy-2-mercapto-6-propylpyrimidine (PTU), copper ions are quantitatively extracted into the phase rich in Triton

Development of a cloud point extraction ...

Jan 10, 2007  A simple and efficient cloud point extraction-spectrofluorimetric method for the determination of copper(II) in different samples has been proposed. The procedure is based on the oxidation of thiamine with copper(II) to form highly fluorescent thiochrome, its extraction to Triton X-114 micelles and spectrofluorimetric determination.

Study on the Cloud Point Extraction of Copper(II) from an ...

In the present work, cloud point extraction process is used with bidentate Schiff base chelating ligand, Nsalicylideneaniline (SA or HL), to extract and separate copper (II)

Development of a cloud-point extraction method for copper ...

Development of a cloud-point extraction method for copper and nickel determination in food samples

(PDF) Cloud Point Extraction Spectrophotometric ...

PDF Cloud point extraction is a separation and preconcentration, simplicity, low cost, fast and environmental safety to determination of copper and...

Surfactant-Mediated Cloud Point Extractions: An ...

Cloud point extraction preconcentration and spectrophotometric determination of copper in food and water samples using amino acid as the complexing agent. Journal of Food Composition and Analysis 2010 , 23 (1) , 95-99.

Use of cloud point extraction for removal of nanosized ...

Triton X-114 based cloud point extraction has been demonstrated to be an advantageous approach for the recovery of nanosized copper oxide (NCO) from water. The removal of NCO was influenced by the concentrations of TX-114 and salt, incubation temperature and time, as well as solution pH. With the addition of 0.3% (w/v) Triton X-114, over 88% of the spiked NCO was

Me-BTABr reagent in cloud point extraction for ...

The present paper describes a new cloud point extraction and preconcentration method for copper by the use of 2-[2´-(6-methyl-benzothiazolylazo)]-4-bromophenol (Me-BTABr) reagent as a complexing agent prior to flame atomic absorption spectrometric determination of this metal.

(PDF) Cloud-point extraction, preconcentration and ...

A new, simple and sensitive cloud point extraction procedure was presented for the preconcentration and determination of copper(II) ion in food, water and biological samples. The analyte was complexed with a new synthesized reagent,

Cloud point extraction and flame atomic absorption ...

Dec 30, 2008  A cloud point extraction procedure was presented for the preconcentration of copper(II) ion in various samples. After complexation by 4-(phenyl diazenyl) benzene-1,3-diamine (PDBDM) (chrysoidine), copper(II) ions were quantitatively recovered in Triton X-114 after centrifugation. 0.5ml of methanol acidified with 1.0molL(-1) HNO3 was added to ...

Cloud point extraction of copper, lead, cadmium, and iron ...

A cloud point extraction procedure was optimized for the separation and preconcentration of lead(II), cadmium(II), copper(II), and iron(III) ions in various water and canned food samples. The metal ions formed complexes with 2,6-diamino-4-phenyl-1,3,5-triazine that were extracted by surfactant-rich phases in the nonionic surfactant Triton X-114.

Sensitive Determination Of Copper By Cloud Point ...

Key words: Cloud point extraction, Flame atomic absorption spectrometry, Copper. Introduction Everyone is exposed to trace amounts of copper through air, soil, household dust, food, drinking water and various consumers. Inorganic copper arising from a number of industrial and mining sources occurs in water in the +2 oxidation state1.

CLOUD POINT EXTRACTION FOR THE DETERMINATION OF

A simple cloud point extraction procedure is presented for the preconcentration of copper in various samples. After complexation by 4-hydroxy-2-mercapto-6-propylpyrimidine (PTU), copper ions are quantitatively extracted into the phase rich in Triton X-114 after

Room temperature cloud point extraction: An application to ...

cloud point extraction, spectrophotometry, copper(II), water analysis, surfactant rich phase Abstract. The novel cloud point extraction procedure for preconcentration of copper(II) was discovered. A simple chemical method for initiating the cloud point extraction (CPE) has been proposed.

Study on the Cloud Point Extraction of Copper(II) from an ...

Study on the Cloud Point Extraction of Copper(II) from an Aqueous Sulfate Medium with N,N′-Bis(salicylideneaminoethyl)amine Polydentate Schiff Base into a Nonionic Surfactant Phase Hasnia Reffas, Tayeb Benabdallah,* Mohamed Hadj Youcef, and Hocine Ilikti

{Room temperature cloud point extraction: An application ...

Abstract: The novel cloud point extraction procedure for preconcentration of copper(II) was discovered. A simple chemical method for initiating the cloud point extraction (CPE) has been proposed. The formation of surfactant rich phase in a system containing a nonionic surfactant Triton X-100, copper

Cloud point extraction of copper, lead, cadmium, and iron ...

A cloud point extraction procedure was optimized for the separation and preconcentration of lead(II), cadmium(II), copper(II), and iron(III) ions in various water and canned food samples. The metal ions formed complexes with 2,6-diamino-4-phenyl-1,3,5-triazine that were extracted by surfactant-rich phases in the nonionic surfactant Triton X-114.

Cloud point extraction for the determination of copper in ...

A simple cloud point extraction procedure is presented for the preconcentration of copper in various samples. After complexation by 4-hydroxy-2-mercapto-6-propylpyrimidine (PTU), copper ions are quantitatively extracted into the phase rich in Triton X-114 after centrifugation.

Application of dual-cloud point extraction for the trace ...

An efficient, innovative preconcentration method, dual-cloud point extraction (d-CPE) has been developed for the extraction and preconcentration of copper (Cu 2+ ) in serum samples of different viral hepatitis patients prior to couple with flame atomic absorption spectrometry (FAAS). The d-CPE procedure was based on forming complexes of elemental ions with complexing reagent 1-(2

Cloud Point Extraction for the Determination of Copper ...

Cloud Point Extraction for the Determination of Copper - Free download as PDF File (.pdf), Text File (.txt) or read online for free. chemical

Selective Determination of Copper in Water Samples by ...

The cloud point is formed in the presence of phenol at room temperature. The method was successfully applied to the determination of copper in water samples and a standard reference material. Keywords: Atomic absorption spectroscopy , Cloud point extraction , Copper , Preconcentration ,

Determination of Zinc, Copper, and Mercury in Water ...

In contrary to traditional cloud point extraction, this method does not need heating. To achieve the cloud point in room temperature, the MCPE procedure was carried out in brine. Triton X-114 was employed as a non-ionic surfactant and the analytes were chelated by 4-(2-pyridylazo) resorcinol prior to extraction.

Cloud point extraction for the determination of trace ...

Cloud point extraction for the determination of copper(II) is proposed after the formation of a complex with sulfapyridylazo resorcinol (SPAR) and later measurement by flame atomic absorption spectrometry (FAAS) using Triton X-100 as a surfactant. The surfactant-rich phase was diluted with nitric acid in methanol, prior to FAAS measurement.

Atomic-Absorption Determination of Copper(II) in Water ...

Abstract We study and optimize the conditions for the cloud-point extraction (CPE) preconcentration of Cu(II) in the form of its complex with 6,7-dihydroxy-4-methyl-2-phenylbenzopyrylium chloride in the micellar phase of the nonionic surfactant Triton X-100. The introduction of ammonium benzoate into the system until a pH of 4.5 is reached at a Triton X-100 concentration of 0.4 vol % leads to ...

Use of cloud point extraction for removal of ... - CORE

Triton X-114 based cloud point extraction has been demonstrated to be an advantageous approach for the recovery of nanosized copper oxide (NCO) from water. The removal of NCO was influenced by the concentrations of TX-114 and salt, incubation temperature and time, as well as solution pH.

Separation and Preconcentration of Copper Ion by Micelle ...

Abstract: Cloud point extraction (CPE) has been used for preconcentration of copper after the formation of a complex with 5, 5-diphenylimidazolidine-2-thione-,4-one (thiophenytoin) (DFID) and later analysis by flame atomic absorption spectrometry (FAAS) using octylphenoxypolyethoxyethanol (Triton X-114) as surfactant.